Pat. No. 5,079,266 describe a technique for
https://www.vapingseller.com/doozy-vape-co.-cool-crush-e-liquid-10ml generating acrolein by de-acetalization of a cyclic acrolein glycerol acetal in contact with a non-siliceous catalyst, the benefit of such a method lying in the fact that the reaction is carried out at ambient temperature. Pat. No. 5,216,179 is reproduced, utilizing a 4-liter fastened mattress of Amberlyst 15 acidic resin in a loop reactor having a quantity of forty liters. Pat. No. 5,216,179 is reproduced in order to obtain a mixture containing the cyclic acrolein glycerol acetals, unconverted acrolein and glycerol, and water.
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https://www.vapeyoung.com/air-factory-strawberry-kiwi-60ml-vape-juice an objective of the current invention consists in providing a technology for producing acrolein from glycerol which makes it attainable to keep up excessive reactant partial pressures,
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It has been discovered, completely surprisingly, that it is possible to produce acrolein with out the abovementioned drawbacks by passing a cyclic acrolein glycerol acetal over a catalyst conventionally used for the dehydration of glycerol, the acetal being prepared beforehand from an aqueous resolution of glycerol and acrolein. 100° C. and 300° C., (c) the fuel stream beforehand obtained is shipped over a glycerol dehydration catalyst in a second reactor, so as to supply acrolein, (d) the acrolein produced is separated from the stream derived from step (c), a part of the acrolein being recycled to the unit for manufacturing of acetals of step (a).
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